HuagongsheHuagongshe Chemistry Print Report · For research reference only
m-Chloroperbenzoic acid → HCID 22117406, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | m-Chloroperbenzoic acid | HCID 70297 | — |
| Reactant | HCID 10502131 | HCID 10502131 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 22117406 | HCID 22117406 | — |
Reaction Steps
The reaction of 1-[(2-dimethylaminoethyl)aminocarbonyl]-5,6-dimethyl-9-acetoxy-6H-pyrido-[4,3-b]carbazole with 3-chloroperoxybenzoic acid in dichloromethane at room temperature results in the desired product, m.p.(cap): 120° C. (decomposition).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06162811 |
| Source dataset | uspto-grants-2000_12 |
| ORD ID | ord-b2ea083f83284003b98b315cfd0ac594 |
| Source note | uspto-grants-2000_12 |