m-Chloroperbenzoic acid → HCID 22117406, compound

HRID 1275545Notes

Reaction equation

HRID 1275545 reaction equation
[CH3:1][N:2]([CH3:31])[CH2:3][CH2:4][NH:5][C:6]([C:8]1[C:24]2[C:12](=[C:13]([CH3:30])[C:14]3[N:15]([CH3:29])[C:16]4[CH:17]=[CH:18][C:19]([O:25][C:26](=[O:28])[CH3:27])=[CH:20][C:21]=4[C:22]=3[CH:23]=2)[CH:11]=[CH:10][N:9]=1)=[O:7].[Cl:32]C1C=C(C=CC=1)C(OO)=[O:37]>ClCCl>[ClH:32].[ClH:32].[CH3:31][N:2]([CH3:1])[CH2:3][CH2:4][NH:5][C:6]([C:8]1[C:24]2[C:12](=[C:13]([CH3:30])[C:14]3[N:15]([CH3:29])[C:16]4[CH:17]=[CH:18][C:19]([O:25][C:26](=[O:28])[CH3:27])=[CH:20][C:21]=4[C:22]=3[CH:23]=2)[CH:11]=[CH:10][N+:9]=1[O-:37])=[O:7]

Participants

4

Reactant 2

HCID 70297m-Chloroperbenzoic acidHCID 10502131HCID 10502131, compound

Product 1

HCID 22117406HCID 22117406, compound

Reagents, catalysts & solvents 1

HCID 6344DichloromethaneSolvent

Procedure

The reaction of 1-[(2-dimethylaminoethyl)aminocarbonyl]-5,6-dimethyl-9-acetoxy-6H-pyrido-[4,3-b]carbazole with 3-chloroperoxybenzoic acid in dichloromethane at room temperature results in the desired product, m.p.(cap): 120° C. (decomposition).

Sources & evidence

ORD record
ord-b2ea083f83284003b98b315cfd0ac594
Source dataset
uspto-grants-2000_12
Patent number
US06162811

Reaction notes

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