HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,2,3,4-Tetrahydroisoquinoline → HCID 22117335, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,2,3,4-Tetrahydroisoquinoline | HCID 7046 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | HCID 22117318 | HCID 22117318 | — |
| Product | HCID 22117335 | HCID 22117335 | 46% |
Reaction Steps
According to the procedure described in Example 7, reaction of 4-(3-chloropropylthio)-3-methyl-2-[(2-pyridinylthio)methyl]pyridine dihydrochloride with 1,2,3,4-tetrahydroisoquinoline and potassium carbonate gives the title compound; m.p. hygroscopic; dec. from 58° C.; yield 46% of theory.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06162809 |
| Source dataset | uspto-grants-2000_12 |
| ORD ID | ord-558bb083262d4a39b8024e8be41aa744 |
| Source note | uspto-grants-2000_12 |