HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → 3-Methyl-2-[(4-pyridinylthio)methyl]-4-[5-(4-pyridinyl)-1,5-dithiapentyl]pyridine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | 4-(3-Chloropropylthio)-3-methyl-2-[(4-pyridinylthio)methyl]pyridine | HCID 22117302 | — |
| Reactant | pyridine-4-thiol | HCID 178418431 | — |
| Product | 3-Methyl-2-[(4-pyridinylthio)methyl]-4-[5-(4-pyridinyl)-1,5-dithiapentyl]pyridine | HCID 22117334 | 69% |
Reaction Steps
According to the procedure indicated in Example 5, reaction of 4-(3-chloropropylthio)-3-methyl-2-[(4-pyridinylthio)methyl]pyridine with 4-mercaptopyridine and sodium hydroxide solution yields the title compound; m.p. 116-118° C.; Yield 69% of theory.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06162809 |
| Source dataset | uspto-grants-2000_12 |
| ORD ID | ord-7097de1553204bc790ee244ffd364ff2 |
| Source note | uspto-grants-2000_12 |