HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Phenylpiperazine → HCID 22117308, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Phenylpiperazine | HCID 7096 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 4-(3-Chloropropylthio)-3-methyl-2-[(4-pyridinylthio)methyl]pyridine | HCID 22117302 | — |
| Product | HCID 22117308 | HCID 22117308 | 79% |
Reaction Steps
According to the procedure indicated in Example 7, reaction of 4-(3-chloropropylthio)-3-methyl-2-[(4-pyridinylthio)methyl]pyridine with 1-phenylpiperazine and potassium carbonate and subsequent chromatography on silica gel gives, after crystallization from diisopropyl ether, the title compound; m.p. from 210° C. (dec.); yield 79% of theory.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06162809 |
| Source dataset | uspto-grants-2000_12 |
| ORD ID | ord-33eab2c9418243e59a6bc251e731125e |
| Source note | uspto-grants-2000_12 |