HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 22117339, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 1-[(5-Chloro-2-thienyl)methyl]piperazine | HCID 2455012 | — |
| Reactant | 4-(3-Chloropropylthio)-3-methyl-2-[(4-pyridinylthio)methyl]pyridine | HCID 22117302 | — |
| Product | HCID 22117339 | HCID 22117339 | 79% |
Reaction Steps
According to the procedure indicated in Example 7, reaction of 4-(3-chloropropylthio)-3-methyl-2-[(4-pyridinylthio)methyl]pyridine with [1-(5-chlorothiophen-2-yl)methyl]piperazine and potassium carbonate gives, after crystallization from isopropanol/acetone/conc. hydrochloric acid, the title compound; m.p. 160-162° C., dec.; yield 79% of theory.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06162809 |
| Source dataset | uspto-grants-2000_12 |
| ORD ID | ord-4343c5501e6b409b91bb018637b73ae7 |
| Source note | uspto-grants-2000_12 |