HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl 4-bromobenzoate → HCID 10473217, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl 4-bromobenzoate | HCID 12081 | — |
| Reactant | 3,5,5,8,8-Pentamethyl-5,6,7,8-tetrahydronaphthalen-2-ol | HCID 226690 | — |
| Product | HCID 10473217 | HCID 10473217 | — |
Reaction Steps
In a manner similar to Example 1(a) above, by the reaction of 1.1 g (5 mmol) of 3,5,5,8,8-pentamethyl-5,6,7,8-tetrahydro-2-naphthol with 0.89 g (4.1 mmol) of methyl 4-bromobenzoate, 670 mg (46%) of the expected methyl ester of melting point 133-5° C. were obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06162815 |
| Source dataset | uspto-grants-2000_12 |
| ORD ID | ord-13e177f78eaa48149524165aede1df78 |
| Source note | uspto-grants-2000_12 |