HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl 4-iodobenzoate → HCID 22117425, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl 4-iodobenzoate | HCID 69273 | — |
| Reactant | 3-Bromo-5,5,8,8-tetramethyl-5,6,7,8-tetrahydronaphthalen-2-ol | HCID 10779311 | — |
| Product | HCID 22117425 | HCID 22117425 | — |
Reaction Steps
In the manner similar to Example 1(a), by the reaction of 1 g (3.5 mmol) of 3-bromo-5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-naphthol with 770 mg (2.94 mmol) of methyl 4-iodobenzoate, 700 mg (58%) of the expected methyl ester of melting point 135-6° C. were obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06162815 |
| Source dataset | uspto-grants-2000_12 |
| ORD ID | ord-df6f1e6929ac4804b1d8a4f18a4da11d |
| Source note | uspto-grants-2000_12 |