Ammonium Chloride → HCID 22117681, compound

Participants

Reaction Steps

To a solution of 4-(2-nitrophenoxy)phenol (1.00 g, 4.3 mmol) in ethanol (50 ml) were added an iron powder (1.21 g, 0.022 g-atom) and a solution of ammonium chloride (0.14 g, 2.6 mmol) in water (10 ml), followed by reflux for 2 hours. The insoluble matter was filtered, and the solvent was evaporated under reduced pressure. The residue was dissolved in ethyl acetate, and after drying, the solvent was evaporated under reduced pressure to give 4-(2-aminophenoxy)phenol (0.85 g).

Provenance & Evidence