HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 15887602, compound → HCID 22117680, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 15887602 | HCID 15887602 | — |
| Reactant | Hydrogen chloride-ethyl acetate | HCID 21866389 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 22117680 | HCID 22117680 | — |
Reaction Steps
2-[4-(3-Nitrobenzyloxy)phenoxy]aniline (0.64 g, 1.9 mmol) was dissolved in ethyl acetate (10 ml), and 4 N hydrogen chloride-ethyl acetate solution (1 ml) was added, followed by stirring for 30 minutes. The solvent was evaporated under reduced pressure, and the residue was crystallized from diethyl ether to give the title compound (0.55 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06162832 |
| Source dataset | uspto-grants-2000_12 |
| ORD ID | ord-b3a0cc36d58846c1bff4a7149f384fe6 |
| Source note | uspto-grants-2000_12 |