Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1275686Generated: October 31, 2026

HCID 15887602, compound → HCID 22117680, compound

https://huagongshe.com/reaction/1275686

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 15887602HCID 15887602—
ReactantHydrogen chloride-ethyl acetateHCID 21866389—
SolventEthyl AcetateHCID 8857—
ProductHCID 22117680HCID 22117680—

Reaction Steps

2-[4-(3-Nitrobenzyloxy)phenoxy]aniline (0.64 g, 1.9 mmol) was dissolved in ethyl acetate (10 ml), and 4 N hydrogen chloride-ethyl acetate solution (1 ml) was added, followed by stirring for 30 minutes. The solvent was evaporated under reduced pressure, and the residue was crystallized from diethyl ether to give the title compound (0.55 g).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06162832
Source datasetuspto-grants-2000_12
ORD IDord-b3a0cc36d58846c1bff4a7149f384fe6
Source noteuspto-grants-2000_12