Benzo(B)Thiophene-2-Boronic Acid → 3-Methyl-9-fluorenone

HRID 1275734Notes

Reaction equation

HRID 1275734 reaction equation
[CH:1]1[C:9]2[C:8]3C4C(=CC=3S[C:5]=2[CH:4]=[CH:3][CH:2]=1)C=CC(=O)C=4.S1C(B(O)O)=CC2C=CC=CC1=2.I[C:31]1[CH:39]=[CH:38][CH:37]=[CH:36][C:32]=1[C:33](O)=[O:34]>>[CH3:8][C:9]1[CH:5]=[CH:4][C:3]2[C:33](=[O:34])[C:32]3[C:31]([C:2]=2[CH:1]=1)=[CH:39][CH:38]=[CH:37][CH:36]=3

Participants

4

Reactant 3

HCID 2359Benzo(B)Thiophene-2-Boronic AcidHCID 69412-Iodobenzoic acidHCID 22117579HCID 22117579, compound

Product 1

HCID 5193573-Methyl-9-fluorenone

Procedure

Benzo[b]indeno[1,2-d]thiophen-9-one: from 2-benzo[b]thiopheneboronic acid and 2-iodobenzoic acid following method A.

Sources & evidence

ORD record
ord-9a66b2f7213940498629489114bcb461
Source dataset
uspto-grants-2000_12
Patent number
US06162824

Reaction notes

Loading…