HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triphenylphosphine → HCID 22117256, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triphenylphosphine | HCID 11776 | — |
| Reactant | Methyl 4-bromo-2-(bromomethyl)benzoate | HCID 22031079 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 22117256 | HCID 22117256 | — |
Reaction Steps
The product of step (i) (26.45 g) and triphenylphosphine (11.7 g) in acetonitrile (100 ml) was heated under reflux for 1.5 hours. The solvent was evaporated and the residue triturated with diethyl ether. The precipitate was collected. Yield 22.8 g. Used directly in the next step.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06162808 |
| Source dataset | uspto-grants-2000_12 |
| ORD ID | ord-f26ad50101fb42b3828eaf1257be7d49 |
| Source note | uspto-grants-2000_12 |