HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,4-Dioxane hydrochloride → N-Propyl-N-propoxyamine hydrochloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,4-Dioxane hydrochloride | HCID 20443148 | — |
| Reactant | N-Boc-N-propyl-N-propoxyamine | HCID 22322626 | — |
| Product | N-Propyl-N-propoxyamine hydrochloride | HCID 22322517 | — |
Reaction Steps
N-Boc-N-propyl-N-propoxyamine (5.8 g) was dissolved in 4N HCl/dioxane (10 mL) and stirred at room temperature for 7 hours. The solvent was removed in vacuo and the residue triturated with diethyl ether. The resulting yellow solid (2.1 g) was collected by filtration and washed with diethyl ether.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06162927 |
| Source dataset | uspto-grants-2000_12 |
| ORD ID | ord-27f15a45884d4ca9897fa94cdfaa408c |
| Source note | uspto-grants-2000_12 |