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HRID1276085

反应详情

EQUATION

反应方程式

HRID 1276085 的结构方程式

REACTANTS

反应物

3
结构：CCOC(=O)CBr
HCID7748

Ethyl bromoacetate

C4H7BrO2

结构：CC(C)n1c(=O)n(C)c2cc(-c3ncc(C(F)(F)F)cc3Cl)ccc21
HCID22114840

未命名化合物

结构：CC(C)n1c(=O)[nH]c2cc(-c3ncc(C(F)(F)F)cc3Cl)ccc21
HCID22114855

未命名化合物

PRODUCTS

生成物

1
结构：CCOC(=O)Cn1c(=O)n(C(C)C)c2ccc(-c3ncc(C(F)(F)F)cc3Cl)cc21
HCID22114867

未命名化合物

收率 68%

PROCEDURE

实验过程

In a similar manner to the preparation of 5-(3-chloro-5-trifluoromethylpyridin-2yl)-3-methyl-1-(1-methylethyl)benzimidazol-2-one described above, 2.5 g of 5-(3-chloro-5-trifluoromethyl-pyridin-2yl)-1-(1-methylethyl)benzimidazol-2 -one and 1.23 g of ethyl bromoacetate gave 2.1 g (68%) of colorless crystals. Yield: 68%, m.p.L 125-127° C.