HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 22115827, compound → HCID 22115821, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 22115827 | HCID 22115827 | — |
| Solvent | Methanol | HCID 887 | — |
| Solvent | Palladium | HCID 23938 | — |
| Product | HCID 22115821 | HCID 22115821 | — |
Reaction Steps
2-Methyl-7-nitro-1,2,3,4-tetrahydroisoquinoline hydrochloride was dissolved in methanol and hydrogenated at 50 psi in the presence of a catalytic quantity of 10% Pd-C. After 1 h the mixture was filtered through glass and evaporated to provide 2-methyl-1,2,3,4-tetrahydroisoquinolin-7-ylamine hydrochloride, m.p. 137-138° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06166030 |
| Source dataset | uspto-grants-2000_12 |
| ORD ID | ord-8844821156a943dd9cb750a46fbbd4c6 |
| Source note | uspto-grants-2000_12 |