HuagongsheHuagongshe Chemistry Print Report · For research reference only
Picolyl chloride hydrochloride → HCID 14422702, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Picolyl chloride hydrochloride | HCID 23392 | — |
| Reactant | HCID 10846487 | HCID 10846487 | — |
| Product | HCID 14422702 | HCID 14422702 | — |
Reaction Steps
By the method of Example 10, the title product of Example 9 (5.70 g, 34.3 mmol) and 2-picolyl chloride hydrochloride (5.63 g, 34.3 mmol) were converted to present title product, 4.37 g (41%), m.p. 56-60° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06166031 |
| Source dataset | uspto-grants-2000_12 |
| ORD ID | ord-f8a4b4b9bc4643dfb8473f8f0b9c5318 |
| Source note | uspto-grants-2000_12 |