HuagongsheHuagongshe Chemistry Print Report · For research reference only
Oxalyl chloride → HCID 22116158, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Oxalyl chloride | HCID 65578 | — |
| Reactant | HCID 22116154 | HCID 22116154 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 22116158 | HCID 22116158 | — |
Reaction Steps
Oxalyl chloride (92 mg) was added to (±)-3-[4-[2-[N-(2-benzoxazolyl)-N-methylamino]ethoxy]phenyl]-2-(2-methoxyethoxy)propanoic acid (100 mg) in dichloromethane (2 mL). The mixture was stirred at room temperature for 16 hours and evaporated to dryness to give the title compound as a gum which was used without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06166049 |
| Source dataset | uspto-grants-2000_12 |
| ORD ID | ord-798b0b314db847ccafdc8dcc0d249b08 |
| Source note | uspto-grants-2000_12 |