HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyclobutylamine → Benzene-1,3-disulfonic acid tert-butyl-amide cyclobutylamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyclobutylamine | HCID 75645 | — |
| Reactant | 3-Tert-butylsulfamoyl-benzenesulfonyl chloride | HCID 16793286 | — |
| Product | Benzene-1,3-disulfonic acid tert-butyl-amide cyclobutylamide | HCID 70000986 | — |
Reaction Steps
Using a procedure similar to that described in Preparation E, 4 ml of cyclobutylamine was added to 1 gram (3.9 mmole) of 3-tert-butylsulfamoyl-benzenesulfonyl chloride to give 813 mg of the titled compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06166064 |
| Source dataset | uspto-grants-2000_12 |
| ORD ID | ord-3ee33d8b29be4ce8a227afed9bccae8b |
| Source note | uspto-grants-2000_12 |