Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1276623Generated: October 25, 2026

Methyl 5-iodo-2-isothiocyanatobenzoate → Methyl 5-iodo-2-[(propoxythioxomethyl)amino]benzoate

https://huagongshe.com/reaction/1276623

Reaction equation

Participants

RoleNameHCIDCharge
ReactantMethyl 5-iodo-2-isothiocyanatobenzoateHCID 14663020—
Solvent1-PropanolHCID 1031—
ProductMethyl 5-iodo-2-[(propoxythioxomethyl)amino]benzoateHCID 22116535—

Reaction Steps

The process of claim 10 wherein (a) methyl 2-amino-5-iodobenzoate is treated to form methyl 5-iodo-2-isothiocyanatobenzoate; (b) the methyl 5-iodo-2-isothiocyanatobenzoate is treated with n-propanol to form methyl 5-iodo-2((propoxy-thioxomethyl)-amino)benzoate, and (c) the methyl 5-iodo-2-((propoxythioxomethyl)-amino)benzoate is treated with propylamine.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06166208
Source datasetuspto-grants-2000_12
ORD IDord-588cb0181dad480c8097a4affb913b70
Source noteuspto-grants-2000_12