HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chloroacetyl chloride → HCID 22116584, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chloroacetyl chloride | HCID 6577 | — |
| Reactant | 3H-spiro(isobenzofuran-1,4'-piperidin)-3-one | HCID 9834255 | — |
| Reactant | HCID 12489093 | HCID 12489093 | — |
| Product | HCID 22116584 | HCID 22116584 | — |
Reaction Steps
The title compound, m.p. 228° C. and MS: m/e=473 (M+H+), was prepared in accordance with the general method of example 1 from 5-amino-3-chloro-10,11-dihydro-5H-dibenzo[a,d]cycloheptene, chloroacetyl chloride, spiro[isobenzofuran-1(3H),4'-piperidin]-3-one and Hcl.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06166209 |
| Source dataset | uspto-grants-2000_12 |
| ORD ID | ord-f0a274ad5ac14150835dfa92955761f8 |
| Source note | uspto-grants-2000_12 |