HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 53714761, compound → Benzoic acid, 4-((S)-hydroxy(5-(1H-imidazol-1-yl)-2-methylphenyl)methyl)-3,5-dimethyl-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 53714761 | HCID 53714761 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | Benzoic acid, 4-((S)-hydroxy(5-(1H-imidazol-1-yl)-2-methylphenyl)methyl)-3,5-dimethyl- | HCID 11056808 | — |
Reaction Steps
The compound obtained in Example 5 was treated in the same manner as in Example 2 to give 13.8 g of (S)-4-[α-hydroxy-5-(1-imidazolyl)-2-methylbenzyl]-3,5-dimethylbenzoic acid, melting point 286-288° C. (decomposition), optical rotation [α]D21 -261.5° (c=1.0, dimethylformamide).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06166221 |
| Source dataset | uspto-grants-2000_12 |
| ORD ID | ord-9bed6ae0c4e3406abdefebfb8d05b9ea |
| Source note | uspto-grants-2000_12 |