HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyrrolidine → HCID 23453673, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyrrolidine | HCID 31268 | — |
| Reactant | HCID 23453746 | HCID 23453746 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 23453673 | HCID 23453673 | — |
Reaction Steps
12 mmoles of 3-(2-methoxyphenyl)-5'-methylthio-spiro[bicyclo[2.2.1]-heptane-2,2'-5-pyrroline]hydriodide and 2 g of pyrrolidine in 50 ml of ethanol are refluxed. The solvent is stripped off and the residue obtained is recrystallized from isopropanol. Colorless crystals of melting point 228° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04277470 |
| Source dataset | uspto-grants-1981_07 |
| ORD ID | ord-840bcb1e2b2145c994a7fc9b8ffdc056 |
| Source note | uspto-grants-1981_07 |