Methyl iodide → HCID 86737839, compound

Participants

Reaction Steps

6 mmoles of 3-phenyl-spiro[bicyclo[2.2.1]-hept-5-ene-2,2'-pyrrolidine]-5'-thione are dissolved in 30 ml of acetone, 1 ml of methyl iodide is added and the mixture is refluxed for 10 minutes. After cooling, the precipitate is filtered off. The crystalline compound, which is pure according to a thin layer chromatogram, is further processed immediately.

Provenance & Evidence