HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Acid → HCID 12802474, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | HCID 12802456 | HCID 12802456 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 12802474 | HCID 12802474 | — |
Reaction Steps
In the same manner as Example 14-(I), 426 mg of Z-Tyr-(D)-Ala-Gly-MePhe-NH-NH2 and 0.06 ml of acetic acid are used toproduce 405 mg of the indicated compound (85%). m.p.142°-143°C.; Rf1 =0.33; [α]D27 -31.8°(c=0.4, DMF)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04277394 |
| Source dataset | uspto-grants-1981_07 |
| ORD ID | ord-f641dd65824d451692e0d7321f431baa |
| Source note | uspto-grants-1981_07 |