HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 12698924, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 12698923 | HCID 12698923 | — |
| Product | HCID 12698924 | HCID 12698924 | — |
Reaction Steps
Ethereal hydrogen chloride is added dropwise to a solution of 1.0 g. 1-[(6-methyl-2-naphthoyl)methyl]imidazole in 100 ml. ether until precipitation is complete. The product is filtered, washed with ether, airdried and recrystallized from methanol/acetone to yield 1-[(6-methyl-2-naphthoyl)methyl]imidazole hydrochloride, m.p. 271°-272° C. (decomp).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04277486 |
| Source dataset | uspto-grants-1981_07 |
| ORD ID | ord-b14e71c63a2247f494df5449edc922fa |
| Source note | uspto-grants-1981_07 |