Potassium Carbonate → HCID 12698923, compound

HRID 1277435Notes

Reaction equation

HRID 1277435 reaction equation
Cl.[CH3:2][C:3]1[CH:4]=[C:5]2[C:10](=[CH:11][CH:12]=1)[CH:9]=[C:8]([C:13]([CH2:15][N:16]1[CH:20]=[CH:19][N:18]=[CH:17]1)=[O:14])[CH:7]=[CH:6]2.C(=O)([O-])[O-].[K+].[K+]>CCOCC>[CH3:2][C:3]1[CH:4]=[C:5]2[C:10](=[CH:11][CH:12]=1)[CH:9]=[C:8]([C:13]([CH2:15][N:16]1[CH:20]=[CH:19][N:18]=[CH:17]1)=[O:14])[CH:7]=[CH:6]2

Participants

4

Reactant 2

HCID 11430Potassium CarbonateHCID 12698924HCID 12698924, compound

Product 1

HCID 12698923HCID 12698923, compound

Reagents, catalysts & solvents 1

HCID 3283Diethyl EtherSolvent

Procedure

1-[(6-Methyl-2-naphthoyl)methyl]imidazole hydrochloride (1.0 g.) suspended in 50 ml. of ether is stirred with excess dilute aqueous potassium carbonate solution until the salt is completely dissolved. The organic layer is then separated, washed twice with water, dried over magnesium sulfate and evaporated to yield 1-[(6-methyl-2-naphthoyl)methyl]imidazole.

Workup

  1. dissolutionis completely dissolved
  2. customThe organic layer is then separated
  3. washwashed twice with water
  4. dry with materialdried over magnesium sulfate
  5. customevaporated

Sources & evidence

ORD record
ord-e03d03afe4b144d381929b778782c663
Source dataset
uspto-grants-1981_07
Patent number
US04277486

Reaction notes

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