HuagongsheHuagongshe Chemistry Print Report · For research reference only
(3-Methoxyphenyl)(phenyl)methanone → 3-Hydroxybenzophenone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (3-Methoxyphenyl)(phenyl)methanone | HCID 12451863 | — |
| Solvent | Hydrogen Bromide | HCID 260 | — |
| Product | 3-Hydroxybenzophenone | HCID 83050 | — |
Reaction Steps
0.1 mole of the 3-methoxybenzophenone thus obtained is heated under reflux for 9 hours in 100 ml of 48% hydrobromic acid. When the hydrolysis is finished the product obtained is recrystallised in a mixture of equal volumes of water and alcohol. Yield: 78%. Melting point of the product obtained: 118° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04277497 |
| Source dataset | uspto-grants-1981_07 |
| ORD ID | ord-16ff61732d3e4a0c855bf8d89e434f63 |
| Source note | uspto-grants-1981_07 |