HRID1277437

反应详情

EQUATION

反应方程式

HRID 1277437 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

0.1 mole of the 3-methoxybenzophenone thus obtained is heated under reflux for 9 hours in 100 ml of 48% hydrobromic acid. When the hydrolysis is finished the product obtained is recrystallised in a mixture of equal volumes of water and alcohol. Yield: 78%. Melting point of the product obtained: 118° C.

WORKUP

后处理

  1. temperatureis heated
  2. customobtained
  3. customis recrystallised in a mixture of equal volumes of water and alcohol
  4. customMelting point of the product obtained
  5. custom118° C.