HuagongsheHuagongshe Chemistry Print Report · For research reference only
A 643C → 2-Amino-N-(1,1-dimethylhexyl)acetamide hydrogen fumarate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | A 643C | HCID 128299 | — |
| Reactant | Fumaric Acid | HCID 444972 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 2-Amino-N-(1,1-dimethylhexyl)acetamide hydrogen fumarate | HCID 23454130 | — |
Reaction Steps
A solution of fumaric acid (12.6 g) in cold methanol (585 mls) was stirred and 2-amino-N-(1,1-dimethylhexyl)acetamide (18.47 g) added to give a clearsolution which rapidly deposited a crystalline solid. After standing at 0° C. for 4 hours this solid was filtered off, washed with ethanol and dried in vacuo, m.p. 154° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04277498 |
| Source dataset | uspto-grants-1981_07 |
| ORD ID | ord-4b82a8312e264f3d80ebbce3c5747447 |
| Source note | uspto-grants-1981_07 |