Hydrochloric Acid → HCID 23452868, compound

HRID 1277590Notes

Reaction equation

HRID 1277590 reaction equation
[C:1]([C:5]1[CH:6]=[C:7]([CH:25]=[C:26]([C:31]([O:33]C)=[O:32])[C:27]=1[N+:28]([O-:30])=[O:29])[O:8][CH2:9][C:10]([N:12]([CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH3:24])[CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH3:18])=[O:11])([O:3]C)=[O:2].[OH-].[Na+].Cl>C(O)C>[C:31]([C:26]1[CH:25]=[C:7]([CH:6]=[C:5]([C:1]([OH:3])=[O:2])[C:27]=1[N+:28]([O-:30])=[O:29])[O:8][CH2:9][C:10]([N:12]([CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH3:18])[CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH3:24])=[O:11])([OH:33])=[O:32]

Participants

5

Reactant 3

HCID 313Hydrochloric AcidHCID 14798Sodium HydroxideHCID 23452884HCID 23452884, compound

Product 1

HCID 23452868HCID 23452868, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

A solution of crude (3,5-dicarbomethoxy-4-nitrophenoxy)-N,N-dihexylacetamide in ethanol is treated with aqueous sodium hydroxide (3 equivalents) at room temperature for 15 min. After this time the reaction is poured into cold dilute hydrochloric acid. The diacid product which precipitates is collected and washed well with water; m.p. 180°-184° C.

Workup

  1. customThe diacid product which precipitates
  2. customis collected
  3. washwashed well with water

Sources & evidence

ORD record
ord-285f428d5c55428dbfc9dd11073e07be
Source dataset
uspto-grants-1981_07
Patent number
US04278598

Reaction notes

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