Acetic Anhydride → HCID 23452998, compound

Participants

Reaction Steps

Dry dioxan (80 ml) was added to 6-(1-aminomethyl)-2-benzyl-3-methyl-1,2,4-triazin-5(4H)-one (4.34 g) and the cloudy suspension stirred at room temperature was treated with acetic anhydride (1.9 ml). The mixture was stirred for 2 hours then concentrated to a brown solid. Recrystallisation from ethanol-ether afforded the acetamide, 3.1 g, m.p. 196°-203°.

Provenance & Evidence