HuagongsheHuagongshe Chemistry Print Report · For research reference only
Oxalyl chloride → 2-Trifluoromethylhexanoyl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Oxalyl chloride | HCID 65578 | — |
| Reactant | 2-Trifluoromethylhexanoic acid | HCID 15745193 | — |
| Product | 2-Trifluoromethylhexanoyl chloride | HCID 20285947 | 90% |
Reaction Steps
2-Trifluoromethylhexanoic acid (2.3 g.) was added dropwise to 10 g. oxalyl chloride (10 g.) and the mixture heated to reflux for 2 hours. Distillation of the reaction mixture after this time yielded 2-trifluoromethylhexanoyl chloride (2.27 g.; 90%), b.p. 67°-70°/43 mmHg.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04256911 |
| Source dataset | uspto-grants-1981_03 |
| ORD ID | ord-30039d14f8c14445b8190fb9e7e5b2b3 |
| Source note | uspto-grants-1981_03 |