HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonium Hydroxide → 2-Iodobenzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonium Hydroxide | HCID 14923 | — |
| Reactant | 2-Iodobenzoyl chloride | HCID 69112 | — |
| Product | 2-Iodobenzamide | HCID 77529 | — |
Reaction Steps
A total of 50 ml of a 15 M ammonium hydroxide solution was reacted with 15 g o-iodobenzoyl chloride for 20 minutes. The crude product was recovered as in Example 1. The product was recrystallized from ethanol to yield 7.8 g of o-iodobenzamide, m.p. 187°-189°, Rf 0.63.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04279887 |
| Source dataset | uspto-grants-1981_07 |
| ORD ID | ord-73879bd1802840bea979c0bba468c15c |
| Source note | uspto-grants-1981_07 |