HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzene → N-cyclohexyl-2-iodobenzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzene | HCID 241 | — |
| Reactant | Cyclohexylamine | HCID 7965 | — |
| Reactant | 2-Iodobenzoyl chloride | HCID 69112 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | N-cyclohexyl-2-iodobenzamide | HCID 774524 | — |
Reaction Steps
In accordance with the procedure of Example 3, 12.1 g of cyclohexylamine was reacted with 8.0 g of o-iodobenzoyl chloride in 20 ml of tetrahydrofuran. There was obtained by recrystallization from benzene 5.7 g of fine white crystals of N-cyclohexyl-o-iodobenzamide, m.p. 148°-149°, Rf 0.74.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04279887 |
| Source dataset | uspto-grants-1981_07 |
| ORD ID | ord-30d02f69c90c46a4bc2ac1f1ba84d41b |
| Source note | uspto-grants-1981_07 |