HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Chloride → HCID 962071, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Chloride | HCID 5234 | — |
| Reactant | Morpholine | HCID 8083 | — |
| Reactant | 2-Iodobenzoyl chloride | HCID 69112 | — |
| Reactant | Benzene hexane | HCID 110624 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 962071 | HCID 962071 | — |
Reaction Steps
A solution of 15 ml of morpholine in 30 ml of tetrahydrofuran was reacted with a solution of 8.0 g o-iodobenzoyl chloride in 20 ml tetrahydrofuran for 10 minutes. The product was obtained in the manner described in Example 3, using saturated NaCl instead of H2O. There was obtained by recrystallization from benzene/hexane 6.8 g of N-o-iodobenzoylmorpholine as hard, translucent crystals, m.p. 86°-87°, Rf 0.73.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04279887 |
| Source dataset | uspto-grants-1981_07 |
| ORD ID | ord-ed8e331728674dffb2c70b8c5d699332 |
| Source note | uspto-grants-1981_07 |