HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonium Hydroxide → 4-Iodobenzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonium Hydroxide | HCID 14923 | — |
| Reactant | 4-Iodobenzoyl chloride | HCID 74373 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | 4-Iodobenzamide | HCID 77561 | — |
Reaction Steps
A total of 20 ml of 15 M ammonium hydroxide was reacted with a solution of 5.4 g p-iodobenzoyl chloride in 25 ml of ether. The crude product was recovered as described in Example 3 and recrystallized from ethanol to yield 3.5 g of p-iodobenzamide as white crystals, m.p. 221°-223°, Rf 0.46.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04279887 |
| Source dataset | uspto-grants-1981_07 |
| ORD ID | ord-6c756c1f5d264869a504fa0636545a07 |
| Source note | uspto-grants-1981_07 |