HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylamine → 4-iodo-N,N-dimethylbenzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylamine | HCID 674 | — |
| Reactant | 4-Iodobenzoyl chloride | HCID 74373 | — |
| Product | 4-iodo-N,N-dimethylbenzamide | HCID 879933 | — |
Reaction Steps
A total of 20 ml of a 40% aqueous solution of dimethylamine was reacted with a solution of 5.4 g p-iodobenzoyl chloride as described in Example 3 and recrystallized from a benzene/hexane mixture to yield 4.9 g N, N-dimethyl-p-iodobenzamide as white crystals, m.p. 113°-115°, Rf 0.69.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04279887 |
| Source dataset | uspto-grants-1981_07 |
| ORD ID | ord-6c9de6e93f0a4e79a4cead7084b2cf2d |
| Source note | uspto-grants-1981_07 |