HRID1278048

反应详情

EQUATION

反应方程式

HRID 1278048 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

Hydrogenate 21.5 g of 2-(4-bromobenzylidene)-1-methylpyrrolidine in 400 ml of ethanol with platinum on activated charcoal/hydrogen. Filter out the catalyst, concentrate the filtrate and distil the residue to obtain 18.5 g (85% of theory) of the title compound (b.p. 70° at 0.001 mm of Hg).

WORKUP

后处理

  1. filtrationFilter out the catalyst
  2. concentrationconcentrate the filtrate
  3. customdistil the residue