HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(4-Bromobenzylidene)-1-methylpyrrolidine → HCID 23452593, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(4-Bromobenzylidene)-1-methylpyrrolidine | HCID 53833314 | — |
| Catalyst | HCID 178506450 | HCID 178506450 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 23452593 | HCID 23452593 | — |
Reaction Steps
Hydrogenate 21.5 g of 2-(4-bromobenzylidene)-1-methylpyrrolidine in 400 ml of ethanol with platinum on activated charcoal/hydrogen. Filter out the catalyst, concentrate the filtrate and distil the residue to obtain 18.5 g (85% of theory) of the title compound (b.p. 70° at 0.001 mm of Hg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04279918 |
| Source dataset | uspto-grants-1981_07 |
| ORD ID | ord-26f51f375edd4c238f0e1cedb920edf8 |
| Source note | uspto-grants-1981_07 |