HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Bromohexane → HCID 23452539, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Bromohexane | HCID 8101 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 2-(4-Chlorobenzyl)pyrrolidine | HCID 5138807 | — |
| Solvent | Methyl Ethyl Ketone | HCID 6569 | — |
| Product | HCID 23452539 | HCID 23452539 | — |
Reaction Steps
Boil 5 g of 2-(4-chlorobenzyl)pyrrolidine, 3.53 g of anhydrous potassium carbonate, 4.6 g of 1-bromohexane and 50 ml of ethyl methyl ketone under reflux for 18 hours. Work up according to the procedure o Example 67 to obtain 5.82 g (81% of theory) of the title compound as a colorless liquid of b.p. 110° to 112° at 0.005 mm of Hg.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04279918 |
| Source dataset | uspto-grants-1981_07 |
| ORD ID | ord-1193b2d7d4c64e64b9fd2b35f3c590c3 |
| Source note | uspto-grants-1981_07 |