HRID1278071

反应详情

EQUATION

反应方程式

HRID 1278071 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

Add a solution of 0.78 g of acetyl chloride in 5 ml of benzene dropwise to a solution of 1.9 g of 2-(4-aminobenzyl)-1-methylpyrrolidine and 1 g of triethylamine in 10 ml of benzene. After one hour, concentrate the resulting reaction mixture. Then take it up with water and diethyl ether. Collect the organic phase and concentrate it to obtain the title compound as a yellowish oil.

WORKUP

后处理

  1. concentrationconcentrate
  2. customthe resulting reaction mixture
  3. customCollect the organic phase
  4. concentrationconcentrate it