HRID1278071
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
AUXILIARIES
试剂、催化剂与溶剂
PROCEDURE
实验过程
Add a solution of 0.78 g of acetyl chloride in 5 ml of benzene dropwise to a solution of 1.9 g of 2-(4-aminobenzyl)-1-methylpyrrolidine and 1 g of triethylamine in 10 ml of benzene. After one hour, concentrate the resulting reaction mixture. Then take it up with water and diethyl ether. Collect the organic phase and concentrate it to obtain the title compound as a yellowish oil.
WORKUP
后处理
- concentrationconcentrate
- customthe resulting reaction mixture
- customCollect the organic phase
- concentrationconcentrate it