Water → HCID 23452555, compound

Participants

Reaction Steps

Stir 0.8 g of 2-(4-chlorobenzyl)-1-[3-(4-fluorobenzoyl)propyl]pyrrolidine at room temperature for 3 hours with 0.5 g of sodium borohydride in 8 ml of methanol/2 ml of water. Concentrate the resulting reaction mixture and then take up the concentrate with water/diethyl ether. Dry the ethereal phase over sodium sulfate and distil off the solvent to obtain the title compound as light-brown viscous oil.

Provenance & Evidence