HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrazine → Veratrohydrazide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrazine | HCID 9321 | — |
| Reactant | Methyl 3,4-Dimethoxybenzoate | HCID 16522 | — |
| Solvent | Water | HCID 962 | — |
| Product | Veratrohydrazide | HCID 1530859 | — |
Reaction Steps
A mixture of 9.8 g (0.05 mol) of methyl 3,4-dimethoxybenzoate and 15 ml of 85% water containing hydrazine was refluxed for 2.5 hours with stirring. The reaction mixture was cooled and the crystals formed were recovered by filtration and washed with water to provide 3,4-dimethoxybenzoic acid hydrazide. The yield was quantitative.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04279982 |
| Source dataset | uspto-grants-1981_07 |
| ORD ID | ord-347cd166ced1414490107c6db4607ad9 |
| Source note | uspto-grants-1981_07 |