HRID1278189

反应详情

EQUATION

反应方程式

HRID 1278189 的结构方程式

PROCEDURE

实验过程

A solution is made in an inert organic solvent of 2-chloro-6-fluorobenzamidocarboxylic acid, 4-nitrophenyl ester, and 5-trifluoromethyl-2-aminopyridine. The temperature of the reaction mixture is raised, and the mixture is stirred for a period of time. The mixture is then evaporated under vacuum, and the product named in the heading above, identical to the product of Example 4, is isolated and purified by recrystallization.

WORKUP

后处理

  1. temperatureThe temperature of the reaction mixture is raised
  2. customThe mixture is then evaporated under vacuum
  3. customis isolated
  4. custompurified by recrystallization