HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrogen Peroxide → HCID 70527488, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrogen Peroxide | HCID 784 | — |
| Reactant | HCID 12766251 | HCID 12766251 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 70527488 | HCID 70527488 | — |
Reaction Steps
A mixture of 0.90 g. of 3-bromo-7-(3-pyridyl)pyrazolo[1,5-a]pyrimidine, 25 ml. of glacial acetic acid and 5 ml. of 30% hydrogen peroxide is heated on a steam bath for 4 hours. The mixture is filtered and the solid recrystallized from ethanol to give 0.40 g. of the product of the example, m.p. 280°-284° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04281000 |
| Source dataset | uspto-grants-1981_07 |
| ORD ID | ord-e40823577067435fa05d5cdcb232094f |
| Source note | uspto-grants-1981_07 |