HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(Dimethylamino)ethanol → HCID 21163094, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(Dimethylamino)ethanol | HCID 7902 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | Hydride | HCID 166653 | — |
| Reactant | ETHYL 7-(PYRIDIN-3-YL)PYRAZOLO[1,5-A]PYRIMIDINE-3-CARBOXYLATE | HCID 11196438 | — |
| Product | HCID 21163094 | HCID 21163094 | — |
Reaction Steps
To a mixture of ethyl 7-(3-pyridyl)pyrazolo[1,5-a]pyrimidine-3-carboxylate in 2-dimethylamino ethanol is added sodium hydride. After the hydride is reacted the mixture is heated on a steam bath for 6 hours. The solvent is removed and the residue acidified with dilute acetic acid to give the product of the example.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04281000 |
| Source dataset | uspto-grants-1981_07 |
| ORD ID | ord-c1a664971f7d424facbde7b8cddcf8d7 |
| Source note | uspto-grants-1981_07 |