HuagongsheHuagongshe Chemistry Print Report · For research reference only
Glycol monoethyl ether → HCID 21163083, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Glycol monoethyl ether | HCID 8076 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | Hydride | HCID 166653 | — |
| Reactant | ETHYL 7-(PYRIDIN-3-YL)PYRAZOLO[1,5-A]PYRIMIDINE-3-CARBOXYLATE | HCID 11196438 | — |
| Product | HCID 21163083 | HCID 21163083 | — |
Reaction Steps
To a mixture of ethyl 7-(3-pyridyl)pyrazolo[1,5-a]pyrimidine-3-carboxylate and 2-ethoxyethanol is added sodium hydride. After the hydride is reacted, the mixture is heated on a steam bath for 12 hours. The solvent is removed and the residue is acidified with dilute acetic acid to give the product of the example.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04281000 |
| Source dataset | uspto-grants-1981_07 |
| ORD ID | ord-990130447918491cb3a08531fd5ef381 |
| Source note | uspto-grants-1981_07 |