Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Dimethylformamide dimethyl acetal → 3-Dimethylamino-1-(6-methyl-2-pyridyl)-2-propen-1-one
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Dimethylformamide dimethyl acetal | HCID 78373 | — |
| 반응물 | 2-Acetyl-6-methylpyridine | HCID 138872 | — |
| 생성물 | 3-Dimethylamino-1-(6-methyl-2-pyridyl)-2-propen-1-one | HCID 53880193 | — |
반응 단계
A mixture of 25.0 g of 2-acetyl-6-methylpyridine and 35 ml. of N,N-dimethylformamide dimethylacetal is refluxed for 16 hours. The mixture is cooled and filtered to give 3-dimethylamino-1-(6-methyl-2-pyridyl)-2-propen-1-one as crystals, m.p. 97°-98° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04281000 |
| 출처 데이터셋 | uspto-grants-1981_07 |
| ORD ID | ord-6a557c30da95423492744838b3851c84 |
| 출처 메모 | uspto-grants-1981_07 |