HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Propen-1-one, 3-(dimethylamino)-1-(4-pyridinyl)- → HCID 12766263, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Propen-1-one, 3-(dimethylamino)-1-(4-pyridinyl)- | HCID 714531 | — |
| Reactant | HCID 178510443 | HCID 178510443 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 12766263 | HCID 12766263 | — |
Reaction Steps
A mixture of 1.12 g. of 3-dimethylamino-1-(4-pyridyl)-2-propen-1-one and 0.69 g. of 3-aminopyrazole-4-carbonitrile in 25 ml. of glacial acetic acid is refluxed 6 hours. The solvent is removed under reduced pressure and the product worked up as for Example 53 to give 0.60 g. of crystals, m.p. 137°-138° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04281000 |
| Source dataset | uspto-grants-1981_07 |
| ORD ID | ord-2dadd8ee0f3a481fafc9b6286402374f |
| Source note | uspto-grants-1981_07 |