HRID1278247

反应详情

EQUATION

反应方程式

HRID 1278247 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

To a mixture of 0.01 mole of 7-(4-pyridyl)pyrazolo[1,5-a]pyrimidine in cold dichloromethane is added 0.011 mole of N-chlorobenzotriazole. The mixture is stirred at room temperature for one hour and heated on a steam bath for 15 minutes. The product is worked up as for Example 62 to give the product of the example, m.p. 183°-184° C.

WORKUP

后处理

  1. temperatureheated on a steam bath for 15 minutes
  2. customto give the product of the example, m.p. 183°-184° C.